Category: HPLC, FPLC, & LC/MS | Subcategory: LC-MS / LC-MS/MS
AB Sciex API 3200 LC/MS/MS With Shimadzu HPLC System, Gerstel MPS 3C, And Peak Scientific Nitrogen Generator
ITEM: 31333
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This AB Sciex API 3200 LC/MS/MS liquid chromatography/mass spectrometry system includes an AB Sciex API 3200 series mass spectrometer, Shimadzu HPLC System, Gerstel MPS 3C, And Peak Scientific Gas Generator.
The API 3200 LC-MS/MS system is a fully-integrated triple quadrupole mass spectrometer built using premier technology that combines sensitivity and selectivity with ruggedness and reliability, all in a compact package. It features the Turbo V ion source with plug-and-play probes that let you analize an extended range of compounds over a wide range of flow rates.
The innovative Turbo V ion source efficiently ionizes compounds over a wide range of flow rates, virtually eliminating cross-contamination, even with large sample loads. The patented LINAC collision cell technology delivers superior MS/MS performance allowing faster scan times without compromising sensitivity or mass spectral quality.
Ideal for a variety of applications including proteomics, drug discovery, drug development, contaminant testing, or forensic studies, the 3200 improves productivity by delivering a single-system solution with best-in-class technical performance.
Specifications: | |
Scanning Range | Quadrupole mode: 5 to 2000 m/z LIT mode: 50 to 1700 m/z |
Dimensions | 42" W x 20" D x 27" H (106.7 x 50.8 x 68.6 cm) |
Weight | 330 lbs. (150 kg) |
Detector Type | Pulse Counting CEM |
Dynamic Range | 5 orders of magnitude |
Ionization Sources | TurboIonSpray, APCI, DuoSpray, PhotoSpray |
Mass Accuracy / Stability | 0.1 Da over 8 hours and 0.15 Da over 24 hours |
Mass Range | 5-1,700 (Quad); 50-1,700 (LIT) |
Polarity Switching Time | 700 ms |
Scan Speed (Quad) | 24,000 Da/sec |
Scan Types | Q1 MS, Q3 MS, Product Ion, Precursor Ion, Neutral Loss or Gain, MRM, EMS, EPI, ER, MS3, TripleTrap |
Operating Altitude | Up to 2000 m (6560 feet) above sea level |
Ambient Temperature* | 5°C (41°F) to 40°C (104°F) |
Relative Humidity | 80% for temperatures up to 31°C (88°F), decreasing lineraly to 50% at 40°C (104°F) |
Mains Supply Voltage Fluctuations | ±10% of the nominal voltage |
Pollution Degree | Pollution Degree 2 |
*Over time, the temperature must remain within a range of 4 °C (7.2 °F), with the rate of the change in temperature not exceeding 2°C (3.6°F) per hour. Ambient temperature fluctuations exceeding the limits might result in mass shifts in spectra.
Features:
- The standard Turbo V ion source provides the plug-and-play TurboIonSpray probe and APCI probe, a durable ceramic interface, and compatibility with high flow rates
- Additional compatible ion sources, including the DuoSpray™ ion source, PhotoSpray ion source, and NanoSpray III ion source components, provide further flexibility
- Scanning in a mass range of m/z 5 to 2000 in quadrupole mode and m/z 50 to 1700 in LIT mode
- LINAC® collision cell eliminates cross-talk and allows for multi-component analysis during an LC run
- Integrated switching valve and integrated syringe pump provide convenient sample introduction flexibility
- Compatible with metabolite ID software, which automates metabolite identification, providing rapid, high-confidence results from experiments
- Safe fluids to be used include Methanol, acetonitrile, water, formic acid, and ammonium acetate
The Shimadzu Prominence HPLC System includes:
- CTO 20A Column Oven
- (2) LC-20AD Pumps
- DGU-20A3 Degasser
- CBM-20A Communications Bus Module
- FCV-11AL Valve Unit
The Shimadzu CTO-20A Column Oven is a forced air-circulation-type column oven. The CTO-20A allows you to regulate the temperature in a range going from 10 deg. C above room temperature to 85 deg. C. Using an electronic cooler, can regulate the temperature in a large range going from 10 deg. C below room temperature to 85 deg. C.
The Shimadzu LC-20AD Solvent Delivery Unit offers the most stable solvent delivery performance in the world. The unit achieves pulse-free solvent delivery with an automatic pulsation-correction mechanism and high-speed micro plunger drive. Flow-rate accuracy and precision in the micro-flow rate region have been improved with the addition of a new type of check valve and modifications to the solvent delivery control method. New and improved plunger seal materials ensure robust, long-lasting performance.
Solvent Delivery Unit Specifications: | |
Solvent Delivery Method | Parallel-type double plunger |
Plunger Capacity | 10µL |
Maximum Discharge Pressure | 40MPa |
Flow-rate Setting Range | 0.0001 to 10.0000 mL/min. |
Flow-rate Accuracy | No more than 1% or 0.5µL/min., whichever is greater (0.01 to 2 mL/min.) |
Flow-rate Precision | No more than 0.06% RSD or 0.02 min SD, whichever is greater |
Pulsation | 0.1 MPa (for water at 1.0 mL/min. and 7MPa) |
Plunger Rinsing Mechanism | Manual rinsing or automatic rinsing using optional product |
Safety Measures | Liquid-leakage sensor, high-pressure/low-pressure limits |
Operating Temperature Range | 4°C to 35°C |
Dimensions | 10.23" W x 16.53" D x 5.5" H (26 x 42 x 14 cm) |
Weight | 22 lbs. (10 kg) |
Power100 VAC, 150 VA, 50/60 Hz |
Shimadzu DGU-20A3 Degasser Specifications: | |
Degassing Performance | UV absorption difference with and without degasser is over 300 mAU (using UV absorption detector, wavelength 210 nm, sensitivity 0.5 AU, flowing Methanol saturated with dissolved Oxygen (HPLC grade) at 25°C with 1 ml/min) |
Number of flow lines | 3 |
Max. Operating Flow Rate | 20 mL/min per flow line (using deionised water - applicable range varies depending on the solvent being delivered) |
Internal capacity | 380µL per flow line |
Pressure Resistance | 98 kPa (1 kgf/cm2) or less (nly when suctioning with the delivery unit. Pressurized delivery to the degasser is prohibited.) |
Tubing | 3 mm O.D. x 1.5 mm I.D. PTFE tubing |
Materials Contacting Solvents | Special synthetic polymers designed for all solvents (degassing membrane), PEEK (connector joints) |
External Output | When system self-diagnostics detects an abnormality, a signal is output to the external terminal (ALARM) |
Self-cleaning | Includes mechanism that extends vacuum pump life by drawing in air when the vacuum pump is running |
Dimensions | 10.24" W x 16.54" D x 2.83" H (26 x 42 x 7.2 cm) |
Weight | 11 lbs. (5 kg) |
Operating Conditions | 4 - 35°C, 20 - 85% humidity |
Power supply | +24 V (powered via connection by remote cable to delivery unit) |
The Shimadzu CBM-20A Communications Bus Module is the world's first Web-based HPLC system controller. With a data buffering function, the CBM-20A acts as an interface for connecting LC workstations, network-client computers, and analytical instruments via Ethernet.
Features:
- Set-up, control and monitor HPLC remotely
- Up to eight modules can be connected
- Equipped with Web-control functions it allows for system control, monitoring, and maintenance information via the internet
- Auto-purge, user intervention is not required to open or close the drain valve
Specifications: | |
Number of Connectable Units | 8 |
Connectable Unit Capability | Solvent Delivery: 4 max Autosamplers: 1 Column Ovens: 1 Detectors: 2 (max.) Fraction Collectors: 1 Sub-controllers: 2 (max.) |
Event I/O | 4 inputs, 4 outputs |
Analog Boards | Up to 2 boards can be mounted |
Operating Temperature Range | 4°C to 35°C |
Dimensions | 10.24" W x 16.54" D x 5.51" H (26 x 42 x 14 cm) |
Weight | 12.13 lbs. (5.5 kg) |
Power | 100 VAC, 50/60HZ, 100VA |
The Gerstel MPS 3C is a multifunctional autosampler and sample preparation robot for GC and GC/MS. The MPS provides modern analytical laboratories high throughput, high performance and unparalleled flexibility.
The Peak Scientific Nitrogen Generator, Model NM20ZA, is designed to operate LC/MS analyzers by producing the required rates, purities and pressures for source and exhaust gas. Utilizing separation technology to selectively remove oxygen, moisture and other gases.
Features:
- Reassurance – Generator performs 24/7, if required
- Durable – Few moving parts with minimum maintenance requirements
- Single Source Solution – One generator can cater for the requirements of multiple AB SCIEX LCMS
- Quiet – Completely silent in operation
- Mobile – Flexibility to position generator where required, wall- mountable for small labs
- Simple Installation – Generator only needs to be connected to the air source and application
- Economical – More cost effective than any other gas supply method
- Convenient – Gas on demand, no health hazards, no need to worry about running out of gas
- Technical Specification
Specifications: | |
Curtain Gas (Nitrogen) | 5L/min @ 60psi |
Source Gas (Zero Air) | 22L/min @ 100psi |
Exhaust Gas (Air) | 8L/min @ 60psi |
Outlet Pressure | System Set |
Nitrogen Pressure Dewpoint | -40°C/-40°F |
Particles | <0.01 µm |
Suspended Liquids | None |
Outlets | (3) 1/4" |
Pressure Gauges | 3 |
Phthalates | None |
Internal Air Compressor | Yes |
Noise Level | 59db(A) |
Power | 230V, 50/60Hz 5.0A |
Dimensions | 37" W x 27" D x 24" H (94 x 67 x 60 cm) |
Weight | 265 lbs. (120 kg) |
System includes a Varian HS 602 dual-stage rotary vane pump, PC pre-loaded with software, monitor, keyboard, mouse and cables.